Ulrich Schubert: Materials Syntheses

Cover: 9783211999127 | Materials Syntheses | A Practical Guide | Ulrich Schubert (u. a.)

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Sprache: Englisch

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Beschreibung

Materials syntheses are generally more complex than syntheses of inorganic or organic compounds, and specific characterization methods play a more important role. Materials synthesis protocols often suffer from unclarities, irreproducibility, lack in detail and lack in standards. The need to change this situation is the main motivation for this book. A number of detailed protocols has been collected, ranging from organic polymers to carbonaceous and ceramic materials, from gels to porous and layered materials and from powders and nanoparticles to films. Preparation methods include intercalation and flux methods, sol-gel processing, templating methods for porous materials, sonochemistry or spray pyrolysis.

Each contribution provides detailed and unambiguous description of the hardware, specific characteristics of the procedure, scope of applicability as well as methods that unequivocally identify and characterize the material and allow checking whether the synthesis was successful.

Zusammenfassung

First book on detailed materials synthesis protocols
Unambiguous descriptions of hardware, specific synthetic procedures and characterization methods
Helpful manual for laboratory courses in materials chemistry

Inhaltsverzeichnis

-Porous Materials; Organically Modified Monolithic Silica Aerogels; Controlling Size and Morphology of Zeolite L; Zeolite A and ZK-4; Mesostructured Silica Thin Films; Porous Silica Gel by Acid Leaching of Metakaolin.-Layered Materials; Zirconia-Pillared Clays; Montmorillonites with mixed aluminum-lanthanide oxide pillars; Birnessite-Type Manganese Oxide by Redox Precipitation.-Carbon; Templated Carbon from Pyrolysis of Pyrene in Pillared Clay Matrices; Fiberous Carbon from Sepiolite Clay and Propylene. -Nanoparticles; Nanoscale Magnesium Oxide; Copper Nanoparticles in Silica; Copper Nanocrystals; Colloidal Dispersion of Gold Nanoparticles; Nanostructured Pt-doped Tin Oxide Films; Assembly of TOPO-Capped Silver Nanoparticles to Multilayered Films.-Inorganic Gels; Octaphenyloctasilsesquioxane and Polyphenylsilsesquioxane for Nanocomposites; Polysilsesquicarbodiimide Xerogels; Monolithic tin-doped silica glass.-Organic Materials and Polymers; Polyaniline A Conducting Polymer.-Metal Oxides and Sulfides; Sonochemically Prepared Molybdenum Sulfide; Aerosol Spray Synthesis of Porous Molybdenum Sulfide Powder; Doped Manganites; Lithium Manganese Oxide Prepared by Flux Methods.

Erscheinungsjahr:	2010
Fachbereich:	Fertigungstechnik
Genre:	Mathematik , Medizin , Naturwissenschaften , Technik
Rubrik:	Naturwissenschaften & Technik
Medium:	Taschenbuch
Inhalt:	vii 228 S.
ISBN-13:	9783211999127
ISBN-10:	3211999124
Sprache:	Englisch
Herstellernummer:	12949694
Einband:	Kartoniert / Broschiert
Autor:	Schubert, Ulrich Hüsing, Nicola Laine, Richard
Redaktion:	Schubert, Ulrich Hüsing, Nicola Laine, Richard
Herausgeber:	Ulrich Schubert/Nicola Hüsing/Richard Laine
Auflage:	Softcover reprint of hardcover 1st edition 2008
Hersteller:	Springer
Verantwortliche Person für die EU:	Springer Verlag GmbH, Tiergartenstr. 17, D-69121 Heidelberg, juergen.hartmann@springer.com
Maße:	235 x 155 x 13 mm
Von/Mit:	Ulrich Schubert (u. a.)
Erscheinungsdatum:	13.10.2010
Gewicht:	0,365 kg